Quantitative determination of lead in mixtures of lead(ii) halides using solid-state 207Pb NMR spectroscopy

文献信息

发布日期 2006-09-05

DOI 10.1039/B609870C

影响因子 4.616

作者

Alicia Glatfelter, Nicole Stephenson, Shi Bai, Cecil Dybowski, Dale L. Perry

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摘要

We demonstrate a multi-spectrum technique for facile, quantitative determination of lead in solid materials using solid-state 207Pb NMR that avoids the major problem of uniform excitation across a wide spectral range; the method can be employed without chemical separation or other chemical manipulations and without any prior sample preparation, resulting in a non-destructive analysis, and producing results that are in agreement with gravimetric analyses of mixed samples of the lead halides.

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来源期刊

Analyst

CiteScore: 7.8

自引率: 5.6%

年发文量: 653

Analyst publishes analytical and bioanalytical research that reports premier fundamental discoveries and inventions, and the applications of those discoveries, unconfined by traditional discipline barriers.

Quantitative determination of lead in mixtures of lead(ii) halides using solid-state 207Pb NMR spectroscopy

文献信息

期刊推荐

相关文献

Tracking areal lithium densities from neutron activation – quantitative Li determination in self-organized TiO2 nanotube anode materials for Li-ion batteries

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High thermal stability of core–shell structures dominated by negative interface energy

Eu3+-Doped Y3−xNdxAl3O12 garnet: synthesis and structural investigation

The role of electron interfacial transfer in mesoporous nano-TiO2 photocatalysis: a combined study of in situ photoconductivity and numerical kinetic simulation

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Drug–DNA complexation as the key factor in photosensitized thymine dimerization

Partitioning of caffeine in lipid bilayers reduces membrane fluidity and increases membrane thickness

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