![1-[4-(4-Methyl-1H-imidazol-1-yl)phenyl]ethanone structure](https://cnstatic.chemtradehub.com/structs/142/142161-53-3-7f55.webp "1-[4-(4-Methyl-1H-imidazol-1-yl)phenyl]ethanone structure")
ATRP mediated encapsulation of Gibbsite: fixation of the morphology by using a cross-linker
文献信息
发布日期
2017-04-24
DOI
10.1039/C7PY00226B
影响因子
5.582
作者
Olessya P. Loiko, Anne B. Spoelstra, Jan Meuldijk, Johan P. A. Heuts
查看原文
摘要
Using ethylene glycol dimethacrylate (EGDMA) as a cross-linker Gibbsite platelets were successfully encapsulated fully using an ATRP-mediated emulsion polymerisation technique. Previously we reported a “muffin-like” morphology, which was obtained using the same approach without a cross-linker. This morphology was attributed to the mobility of the growing polymeric chains, allowing them to move one side of the platelet during the reaction. The addition of EGDMA reduces this mobility and it is shown that this approach indeed leads to encapsulated Gibbsite. A comprehensive study of the reaction conditions, in particular the cross-linker addition profile and concentration, was carried out in combination with cryo-TEM characterization of the final particle morphology.
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来源期刊
Polymer Chemistry
CiteScore:
8.6
自引率:
7.3%
年发文量:
457
Polymer Chemistry welcomes submissions in all areas of polymer science that have a strong focus on macromolecular chemistry. Manuscripts may cover a broad range of fields, yet no direct application focus is required.
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